In Situ TEM Gas & Heating
An Integrated Approach to TEM Characterisation of Catalysts
It’s widely accepted that nanotechnology is needed to help solve the challenges facing human society today, including the energy crisis and environmental protection. We as the scientific community need to turn this agreement into reality, and an understanding of the nano-world is required to assist in providing solutions to these global challenges. The Climate system enables the nano-world to be investigated in the real-world 1 bar pressure, gas and heating environment.
Nano-Reactor: The smallest known chemical reactor
Based on MEMS technology, the Nano-Reactor is a functional sample carrier that enables the controlled and clean reactive environment for imaging chemical reactions at the nano-scale. Integrated into the Nano-Reactor is the 4-contact micro-heater and micro-sensor for locally controlling the temperature environment from RT to 1,000 °C. As a consumable, the Nano-Reactor ensures a clean experiment and keeps your research at the forefront of technology!
Modular Sample Holder: Removable tip & tubing for clean experiments
A clean environment is essential to in situ microscopy and the modularity of the Sample Holder allows for all components that come into contact with the reaction gases to be replaced or cleaned on-site by the user. This includes the gas tubing, metal tip & lid, O-rings and consumable Nano-Reactor. The holder meets the X-Rays safety requirements of all TEM manufacturers.
Gas Supply Systems: Precise and fast control of your gas experiment
The Gas Supply System is a game changer for TEM catalyst research that integrates all gas control functions into one smooth platform. Optimised for gas flow through the Nano-Reactor, the Gas Supply System Light (Climate G) controls the pressure and flow while the full Gas Supply System (Climate G+) adds dynamic mixing with precise control of gas composition at the sample. The Gas Supply Systems allow for imaging and analysis of catalyst particles reactions at the atomic scale.
Full Integration & Automation: Heating & biasing control from one interface
Impulse software gives researchers complete control over their stimuli. With Impulse, you can easily design your In Situ experiment from your desk. Decide which sample conditions you want to be met at which time and Impulse will do the rest.
During your TEM experiment, Impulse will automatically control the sample environment while you focus on the results. Your experiment design is stored so that you can reliably reproduce your results.
- Drag & drop profile builder: Design & automate your experiment
- Flexible graph interface: Large canvas area for rearrangeable graphs
- Real-time data analysis: Plot Real-time I-V and R-T curves
- Synchronized stimuli data: Correlate between stimuli
- Data integration: Synchronize In Situ with TEM data
Gas Analyzer: Accurate analysis of reaction products
Designed to work flawlessly with the Climate Gas & Heating solution, the DENSsolutions Gas Analyzer enables accurate analysis of gasses produced during chemical reactions within the Nano-Reactor, even in very small amounts.
Static & flow modes
- Nanomaterial Growth